1-苄基-1H-吲哚-2-羧酸合成路线 (共 13 条)
反应条件
1: 58 percent / 1) sodium ethylate; 2) 5N sodium hydroxide / 1) toluene, RT, 20 h; 2) 80-90 deg C, 5-10 min
2: Heating
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参考文献
Baiocchi, Leandro; Giannangeli, Marilena
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1905 - 1909
反应条件
1: 75 percent / diethylphosphorocyanidate, NEt3 / dimethylformamide / 2 h / Ambient temperature
2: 70 percent / AlCl3 / various solvent(s) / 2 h / Ambient temperature
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参考文献
Watanabe; Kobayashi; Nishiura; Takahashi; Usui; Kamiyama; Mochizuki; Noritake; Yokoyama; Murakami
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 5 p. 1152 - 1156
反应条件
1: Et3N; PBu3 / tetrahydrofuran / 20 °C
2: 90 percent / n-Bu3SnH; AIBN / benzene / 2 h / Heating
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参考文献
Bennasar, M.-Lluisa; Roca, Tomas; Ferrando, Francesc
Tetrahedron Letters, 2004 , vol. 45, # 29 p. 5605 - 5609