2,4-二溴噻唑-5-甲醇合成路线 （共 7 条）
反应条件
sodium tetrahydroborate in methanol T=23°C; 2 h;
参考文献
Synthetic Communications, , vol. 25, # 17 p. 2639 - 2645
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 2.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 24 p. 4514 - 4525
反应条件
hydrogen; sodium acetate; palladium on activated charcoal in methanol T=23°C; P=3040 Torr; 10 h;
参考文献
Kerdesky; Seif
Synthetic Communications, 1995 , vol. 25, # 24 p. 4081 - 4086
反应条件
palladium in methanol
反应条件
platinum(IV) oxide; hydrogen; sodium acetate in methanol P=760.051 Torr;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 52, # 4 p. 110 - 113
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in toluene
T=100°C; Suzuki reaction;
参考文献
Pereira, Raquel; Furst, Audrey; Iglesias, Beatriz; Germain, Pierre; Gronemeyer, Hinrich; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4514 - 4525
反应条件
tris(dibenzylideneacetone)dipalladium (0); triphenyl-arsane in 1-methyl-pyrrolidin-2-one
T=70°C; Stille reaction; 24 h;
参考文献
Pereira, Raquel; Gaudon, Claudine; Iglesias, Beatriz; Germain, Pierre; Gronemeyer, Hinrich; De Lera, Angel R.
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 1 p. 49 - 54
