4-羟基-[1,1-联苯]-2-羧酸甲酯合成路线 （共 5 条）
反应条件
1: With CoBr2(1,2-bis(diphenylphosphino)ethane); zinc(II) iodide; zinc in dichloromethane T=20°C; Diels-Alder Cycloaddition; 16 h; Inert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=20°C; 1.5 h; Inert atmosphere; Overall yield = 79 percent; Overall yield = 90.7 mg;
参考文献
Puenner, Florian; Schieven, Justin; Hilt, Gerhard
Organic Letters, 2013 , vol. 15, # 18 p. 4888 - 4891
反应条件
hydrogenchloride 96 h; Ambient temperature;
参考文献
Estenne, Genevieve; Dodey, Pierre; Renaut, Patrice; Leclerc, Gerard
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 500 - 503
反应条件
1: 80 percent / Pd(PPh3)4, 2M aq. NaHCO3 / toluene / 18 h / Heating 2: 80 percent / pyridinium chloride / 4 h / 200 °C 3: 90 percent / HCl gas / 96 h / Ambient temperature View Scheme
参考文献
Estenne, Genevieve; Dodey, Pierre; Renaut, Patrice; Leclerc, Gerard
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 500 - 503
反应条件
1: 80 percent / Pd(PPh3)4, 2M aq. NaHCO3 / toluene / 18 h / Heating 2: 80 percent / pyridinium chloride / 4 h / 200 °C 3: 90 percent / HCl gas / 96 h / Ambient temperature View Scheme
参考文献
Estenne, Genevieve; Dodey, Pierre; Renaut, Patrice; Leclerc, Gerard
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 500 - 503
反应条件
1: 80 percent / pyridinium chloride / 4 h / 200 °C 2: 90 percent / HCl gas / 96 h / Ambient temperature View Scheme
参考文献
Estenne, Genevieve; Dodey, Pierre; Renaut, Patrice; Leclerc, Gerard
Organic Preparations and Procedures International, 1995 , vol. 27, # 4 p. 500 - 503
