O-[2-(乙酰氨基)-2-脱氧-beta-D-吡喃葡萄糖基]-L-丝氨酸合成路线 （共 7 条）
反应条件
methanol; sodium methylate
2 h; Ambient temperature;
参考文献
Paulsen; Hoelck
Carbohydrate research, 1982 , vol. 109, p. 89 - 107
反应条件
hydrogen; palladium on activated charcoal in methanol; acetic acid
4 h; Ambient temperature;
参考文献
Paulsen; Hoelck
Carbohydrate research, 1982 , vol. 109, p. 89 - 107
反应条件
1: 85 percent / 1.) AgCO3, drierite, molecular sieve; 2.) AgClO4 / toluene; CH2Cl2 / 18 h
2: NiCl2*6H2O, H3BO3, NaBH4 / ethanol
3: pyridine
4: 95 percent / H2 / 9.7percent Pd-C / acetic acid; methanol / 3 h / Ambient temperature
5: 94 percent / NaOMe/MeOH / 2 h / Ambient temperature
View Scheme
参考文献
Paulsen; Hoelck
Carbohydrate research, 1982 , vol. 109, p. 89 - 107
反应条件
1: 95 percent / H2 / 9.7percent Pd-C / acetic acid; methanol / 3 h / Ambient temperature
2: 94 percent / NaOMe/MeOH / 2 h / Ambient temperature
View Scheme
参考文献
Paulsen; Hoelck
Carbohydrate research, 1982 , vol. 109, p. 89 - 107
反应条件
1: 54 percent / trimethylsilyl triflate / CH2Cl2 / 0.5 h / -15 - 20 °C
View Scheme
参考文献
Gambert, Ulrike; Thiem, Joachim
Carbohydrate Research, 1997 , vol. 299, # 1-2 p. 85 - 89
反应条件
1: acetic acid; palladium 10 on activated carbon; hydrogen / methanol / 18 h / 1140.08 Torr
2: sodium methylate / methanol / 3 h
View Scheme
参考文献
Martins-Teixeira, Maristela B.; Campo, Vanessa L.; Biondo, Monica; Sesti-Costa, Renata; Carneiro, Zumira A.; Silva, Joao S.; Carvalho, Ivone
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 7 p. 1978 - 1987
反应条件
1: α-N-acetylgalactosaminidase from Aspergillus niger CCIM K2 / 240 h / 35 °C / pH 4.8 / citrate-phosphate buffer; Enzymatic reaction
2: pH 4
View Scheme
参考文献
Weignerova, Lenka; Pelantova, Helena; Manglova, Dana; Michalkova, Klara; Kren, Vladimir
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 150 - 155
