5-甲基-2-(4-甲基苯基)-1,2-二氢-3H-吲唑-3-酮合成路线 (共 1 条)
反应条件
pyridine; aluminum oxide; pentacarbonyliron(0); carbon monoxide; Azobenzene in chlorobenzene
T=180°C; P=105008 Torr; 0.333333 h; other reagent Fe(CO)5/Al2O3 + PdCl2Py2; other temperature: 190, 200, 220 deg C; other pressure: 8 MPa; other time 30 min; Product distribution;
参考文献
Lapidus; Pelrovskii; Manov-Yuvenskii; Zelinsky
Russian Chemical Bulletin, 1996 , vol. 45, # 10 p. 2331 - 2334