反应条件
1: sodium azide / H2O; acetone / 1 h / Ambient temperature
2: H2, HCl / Pd-C / methanol
3: 57.8 percent / HCl / H2O; ethanol / 1.5h, r.t., 2h, reflux
4: 74.1 percent / Raney nickel / ethanol / 1 h / Heating
View Scheme
参考文献
Isomura; Sakamoto; Ito; Homma; Abe; Kubo
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 152 - 165