2,5,8,11,14,17,20-七氧杂二十二烷-22-胺合成路线 (共 2 条)
反应条件
1: With sodium azide in N,N-dimethyl-formamide T=110°C; 3 h; 2: With triphenylphosphine in tetrahydrofuran T=20°C; 18 h; Inert atmosphere;
参考文献
Matsumoto, Sayaka; Iwamoto, Hiroya; Mizutani, Tadashi
Chemistry - An Asian Journal, 2010 , vol. 5, # 5 p. 1163 - 1170
反应条件
1.1: sodium hydroxide / tetrahydrofuran; water / 8 h / Cooling with ice 2.1: sodium azide / N,N-dimethyl-formamide / 3 h / 110 °C 2.2: 18 h / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 5, # 5 p. 1163 - 1170