氮丙啶-1,2-二甲酸 1-苄酯 2-甲酯合成路线 (共 5 条)
反应条件
sulfuric acid; triethylamine in methanol; dichloromethane
反应条件
N-benzyl-N,N,N-triethylammonium chloride in acetonitrile T=20°C; 24 h;
参考文献
Chemical Communications, , # 47 p. 6363 - 6365
反应条件
anhydrous sodium hydrogen carbonate; trifluoroacetic acid in diethyl ether; chloroform; water
反应条件
sodium tetrahydroborate in methanol; tert-butyl alcohol
1 h; Heatingultrasonic irradiation; Yield given;
参考文献
Nurdinov, R.; Liepin'sh, E. E.; Kalvin'sh, I. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 11 p. 1352 - 1357
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 11 p. 1567 - 1573
反应条件
sodium tetrahydroborate in methanol; tert-butyl alcohol
Heating; Title compound not separated from byproducts;
参考文献
Nurdinov, R.; Liepin'sh, E. E.; Kalvin'sh, I. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 11 p. 1352 - 1357
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 11 p. 1567 - 1573