1-(3-氨基-4-甲基苯基)乙酮合成路线 (共 15 条)
反应条件
hydrogen; palladium on activated carbon in ethanol 3 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: WO2003/90912 A1, 2003 ;
Location in patent: Page/Page column 129 ;
WO 03/090912 A1
参考文献
Bristol-Myers Squibb Company
Patent: US2010/215616 A1, 2010 ;
反应条件
1: 18.9 percent / nitration 2: 2.45 g / SnCl2 View Scheme
参考文献
Lutz et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 617,680
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Morgan; Pettet
Journal of the Chemical Society, 1934 , p. 418,420
反应条件
isopropyl alcohol in acetonitrile Irradiation;
参考文献
Kammari, Laxminarayana; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr
Journal of the American Chemical Society, 2010 , vol. 132, # 33 p. 11431 - 11433
参考文献
Sacha; Patel
Journal of the Indian Chemical Society, 1956 , vol. 33, p. 129
反应条件
1: AlCl3 2: aqueous HCl View Scheme
参考文献
Sacha; Patel
Journal of the Indian Chemical Society, 1956 , vol. 33, p. 129
参考文献
Brady; Day
Journal of the Chemical Society, 1934 , p. 114,119
反应条件
sulfuric acid; hydrogen bromide; copper(I) bromide
参考文献
Journal of the Chemical Society, , p. 227,232
Journal of Organic Chemistry, , vol. 12, p. 617,680
反应条件
1: With sulfuric acid in water T=20 - 45°C; Inert atmosphere; 2: With sodium nitrite in water T=0°C; Inert atmosphere; 3: in water 5 h; Inert atmosphereReflux;
参考文献
Helvetica Chimica Acta, , vol. 93, # 7 p. 1261 - 1273
反应条件
1: N2H4+H2O; KOH View Scheme
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1951 , vol. 232, p. 1356
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1951 , vol. 233, p. 627