二(三甲基硅氧基)环丁烯合成路线 (共 48 条)
反应条件
tin(IV) chloride in dichloromethane T=-78°C;
参考文献
Journal of the American Chemical Society, , vol. 106, p. 1759
反应条件
water; tin(IV) chloride 1.) methylene chloride, 15 min, -78 deg C, 15 min, -30 deg C; Yield given. Multistep reaction;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
参考文献
Salauen, J.; Almirantis, Y.
Tetrahedron, 1983 , vol. 39, # 14 p. 2421 - 2428
反应条件
boron trifluoride diethyl etherate; water 1.) CH2Cl2, -78 deg C, 3 h, 2.) -78 deg C to r.t., overnight; Yield given. Multistep reaction;
参考文献
Jenkins; Burnell
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1485 - 1491
反应条件
(i) Br2, CH2Cl2, (ii) H2O; Multistep reaction;
参考文献
Ollivier, J.; Salauen, J.
Tetrahedron Letters, 1984 , vol. 25, # 12 p. 1269 - 1272
反应条件
(i) SnCl4, (ii) Et3N, (iii) H2O; Multistep reaction;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
(i) SnCl4, (ii) Et3N; Multistep reaction;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
(i) SnCl4, (ii) Et3N; Multistep reaction;
参考文献
Nakamura,E. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 4166 - 4167
反应条件
boron trifluoride diethyl etherate in dichloromethane
-78 deg C, 8 h; RT, overnight;
参考文献
Pandey, Bipin; Khire, Uday R.; Ayyangar, Nagaraj R.
Synthetic Communications, 1989 , vol. 19, # 15 p. 2741 - 2748
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-70°C;
参考文献
Nakamura, Eiichi; Shimada, Jun-ichi; Kuwajima, Isao
Journal of the Chemical Society, Chemical Communications, 1983 , # 9 p. 498 - 499