二(三甲基硅氧基)环丁烯合成路线 （共 48 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane
1.5 h;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
titanium tetrachloride in dichloromethane
1 h;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
boron trifluoride diethyl etherate
1.) CH2Cl2, -78 deg C, 20 min, 2.) CH2Cl2, from -78 deg C to RT, overnight; Yield given. Multistep reaction;
参考文献
Liu; Wu; Burnell
Canadian Journal of Chemistry, 1997 , vol. 75, # 6 p. 656 - 664
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
T=-78 - 20°C;
2: With Amberlyst 15; trifluoroacetic acid
10 h; Heating;
参考文献
Gao, Fuye; Burnell, D. Jean
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 356 - 359
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78 - 20°C; Condensation;
参考文献
Reddy, Ravinder S.; Saravanan; Kumar, Pradeep
Tetrahedron, 1998 , vol. 54, # 23 p. 6553 - 6564
反应条件
boron trifluoride diethyl etherate; water
1.) r.t., 3.7 h, 2.) overnight; Yield given. Multistep reaction;
参考文献
Jenkins; Burnell
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1485 - 1491
反应条件
titanium tetrachloride in dichloromethane
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
titanium tetrachloride in diethyl ether
1 h;
参考文献
Shimada,J.; Hashimoto,K.; Kim,B.H.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1759
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=20°C; 5 h;
参考文献
Kreiser, Wolfgang; Wiggermann, Annette; Krief, Alain; Swinnen, Dominique
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7119 - 7122
