反应条件
HCl in tetrahydrofuran; water; toluene stirring (25°C, 15 min), evapn., toluene and H2O addn., air bubbling (10 min), filtering, extg. (H2O), washing (ether), pptn. on KPF6 soln. (H2O) addn. (stirring), filtering, washing (ether), drying (CaSO4, 2 d); chromy. (alumina, Me2CO, 1percent MeOH / Me2CO), evapn., washing (ether), drying (vac.);
参考文献
Hollandsworth, Carl B.; Gary Hollis Jr.; Slebodnick, Carla; Deck, Paul A.
Organometallics, 1999 , vol. 18, # 18 p. 3610 - 3614
