Boc-D-烯丙基甘氨酸合成路线 (共 11 条)
反应条件
sodium hydroxide in methanol; water 3.5 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water 5 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 7 p. 2133 - 2143
反应条件
hydrogenchloride in water
参考文献
Protein and Peptide Letters, , vol. 19, # 12 p. 1245 - 1249
反应条件
1: 99 percent / NaHCO3 / dioxane; H2O / 1 h / 23 °C 2: 99 percent / NaOH / H2O; methanol / 3.5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
1: 99 percent / NaHCO3 / dioxane; H2O / 1 h / 23 °C 2: 99 percent / NaOH / H2O; methanol / 3.5 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 4 p. 656 - 673
反应条件
sodium hydroxide; sodium hydrogencarbonate 1.) reflux, 2.) 1.5 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 117, # 32 p. 8488 - 8489
反应条件
dipyridinium dichromate in N,N-dimethyl-formamide 6 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 4 p. 1275 - 1294
反应条件
1: Zn; AcOH / 70 °C 2: dioxane / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 47, # 19 p. 3311 - 3314
反应条件
1: Et3N, DMAP / CH2Cl2 / 9 h / Ambient temperature 2: 71 percent / NaBH4, MeOH / ethanol / 24 h / Ambient temperature 3: pyridinium dichromate / dimethylformamide / 6 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 53, # 4 p. 1275 - 1294
反应条件
1: dioxane / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 47, # 19 p. 3311 - 3314