反应条件
pyridine; lithium borohydride; chloro-trimethyl-silane; potassium carbonate 1.) THF, r.t., 14 h, 2.) CH2Cl2, -20 deg C, 48 h, 3.) acetone, r.t., 12 h; Yield given. Multistep reaction;
参考文献
Farmer, Jay J.; Attygalle, Athula B.; Smedley, Scott R.; Eisner, Thomas; Meinwald, Jerrold
Tetrahedron Letters, 1997 , vol. 38, # 16 p. 2787 - 2790