(2E)-N-甲氧基-N,4-二甲基-2-戊酰胺合成路线 （共 5 条）
反应条件
isopropylmagnesium chloride in tetrahydrofuran T=-4 - 20°C;
参考文献
Kusama, Hiroyuki; Karibe, Yusuke; Imai, Rie; Onizawa, Yuji; Yamabe, Hokuto; Iwasawa, Nobuharu
Chemistry - A European Journal, 2011 , vol. 17, # 17 p. 4839 - 4848
反应条件
pyridine in chloroform T=20°C; 2.5 h;
参考文献
Shintani, Ryo; Kimura, Takahiro; Hayashi, Tamio
Chemical Communications, 2005 , # 25 p. 3213 - 3214
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Chippindale, Ann M.; Davies, Stephen G.; Iwamoto, Keiji; Parkin, Richard M.; Smethurst, Christian A. P.; Smith, Andrew D.; Rodriguez-Solla, Humberto
Tetrahedron, 2003 , vol. 59, # 18 p. 3253 - 3265
反应条件
1: oxalyl chloride / diethyl ether 2: 94 percent / pyridine / CHCl3 / 2.5 h / 20 °C View Scheme
参考文献
Shintani, Ryo; Kimura, Takahiro; Hayashi, Tamio
Chemical Communications, 2005 , # 25 p. 3213 - 3214
反应条件
sodium hydride; trimethylphosphane 1.) DME, 20 min; 2.) DME, 10 min then 120 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Beney, Chantal; Boumendjel, Ahcene; Mariotte, Anne-Marie
Tetrahedron Letters, 1998 , vol. 39, # 32 p. 5779 - 5780
