2-[(1S,2S)-1-乙基-2-苄氧基丙基]肼甲醛合成路线 （共 4 条）
反应条件
1: (S)-2-(Benzyloxy)-N-(Formylamino)-Propanimine With N,N-bis(trimethylsilyl)acetamide in diethyl ether T=20°C; 0.75 h; 2: ethylmagnesium bromide in diethyl ether T=20°C; Grignard addition;
参考文献
Saksena, Anil K.; Girijavallabhan, Viyyoor M.; Wang, Haiyan; Lovey, Raymond G.; Guenter, Frank; Mergelsberg, Ingrid; Puar, Mohinder S.
Tetrahedron Letters, 2004 , vol. 45, # 44 p. 8249 - 8251
反应条件
1.1: 80 percent / methanol 2.1: bis(trimethylsilyl) acetamide / diethyl ether / 0.75 h / 20 °C 2.2: 62.3 percent / diethyl ether / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 44 p. 8249 - 8251
反应条件
1.1: 94 percent / Red-Al / toluene / 5 h 2.1: 80 percent / methanol 3.1: bis(trimethylsilyl) acetamide / diethyl ether / 0.75 h / 20 °C 3.2: 62.3 percent / diethyl ether / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 44 p. 8249 - 8251
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
参考文献
Saksena, Anil K.; Girijavallabhan, Viyyoor M.; Wang, Haiyan; Lovey, Raymond G.; Guenter, Frank; Mergelsberg, Ingrid; Puar, Mohinder S.
Tetrahedron Letters, 2004 , vol. 45, # 44 p. 8249 - 8251
