N-(2-氯苯亚甲基)-4-甲氧基苯胺合成路线 （共 5 条）
反应条件
sulfuric acid in neat (no solvent) Microwave irradiationSealed tubeGreen chemistry;
参考文献
Suresh; Kamalakkannan; Ranganathan; Arulkumaran; Sundararajan; Sakthinathan; Vijayakumar; Sathiyamoorthi; Mala; Vanangamudi; Thirumurthy; Mayavel; Thirunarayanan
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 101, p. 239 - 248
反应条件
1: 48 percent / CrO3 / acetic acid; acetic acid; acetic anhydride / 0.5 h / Ambient temperature 2: ethanol / 1 h / Heating View Scheme
参考文献
Agracheva, E. B.; Krasnikova, L. Ya.; Gachkovskii, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 10 p. 2307 - 2313,1870 - 1874
反应条件
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran T=0°C; Inert atmosphere; 2: (2-chlorobenzylidene)(4-methoxyphenyl)amine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=0°C; 3 h; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran T=20°C; 3 h;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 16 p. 2925 - 2928
反应条件
1: phenyl-magnesium bromide With ZnCl2*TMEDA in tetrahydrofuran T=0°C; Inert atmosphere; 2: (2-chlorobenzylidene)(4-methoxyphenyl)amine With iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=0°C; 3 h; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran T=20°C; 3 h;
参考文献
Yoshikai, Naohiko; Matsumoto, Arimasa; Norinder, Jakob; Nakamura, Eiichi
Angewandte Chemie, International Edition, 2009 , vol. 48, # 16 p. 2925 - 2928
反应条件
2-(4'-carboxyphenyl)benzothiazoline; trifluoroacetic acid in acetonitrile
T=20°C; 23 h; Inert atmosphere;
参考文献
Zhu, Chen; Akiyama, Takahiko
Tetrahedron Letters, 2012 , vol. 53, # 4 p. 416 - 418
