2-溴-5-羟基甲基苯甲醚合成路线 (共 6 条)
反应条件
Sodium bromate; sodium hydrogensulfite in water; acetonitrile T=20°C; 1.5 h;
参考文献
Speicher, Andreas; Backes, Timo; Grosse, Stefan
Tetrahedron, 2005 , vol. 61, # 49 p. 11692 - 11696
反应条件
borane in tetrahydrofuran; methanol
参考文献
Smithkline Beckman Corporation
Patent: US4707483 A1, 1987 ;
反应条件
n-butyllithium; 1,2-dibromo-1,1,2,2-tetrafluoroethane; potassium tert-butylate in tetrahydrofuran; hexane -78 deg C; -78 deg C, 4.5 h; -78 deg C, 10 min;
参考文献
Baker, Robert W.; Liu, Song; Sargent, Melvyn V.; Skelton, Brian W.; White, Allan H.
Australian Journal of Chemistry, 1997 , vol. 50, # 8 p. 831 - 840
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-40°C;
参考文献
Jiang, Juan; Sun, Bin; Wang, Yan-Yan; Cui, Min; Zhang, Li; Cui, Chang-Zhi; Wang, Yan-Feng; Liu, Xi-Gong; Lou, Hong-Xiang
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 7 p. 2382 - 2391
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 4 h;
参考文献
Zhang, Qin; Zhong, Ying; Yan, Lin-Na; Sun, Xun; Gong, Tao; Zhang, Zhi-Rong
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 3 p. 1010 - 1014
反应条件
toluene-4-sulfonic acid in dichloromethane T=20°C; 16 h;
参考文献
Tetrahedron, , vol. 61, # 49 p. 11692 - 11696