(2E,4E)-2,4-己二烯-1-醇合成路线 （共 34 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 3 h;
参考文献
Paquette,L.A.; Crouse,G.D.; Sharma,A.K.
Journal of the American Chemical Society, 1982 , vol. 104, p. 4411
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Heating;
参考文献
Gajewski,J.J.; Jurayj,J.; Kimbrough,D.R.
Journal of the American Chemical Society, 1987 , vol. 109, p. 1170
反应条件
chloro-trimethyl-silane; copper/silver activated zinc in methanol; water T=20°C; 1.5 h; stereoselective reaction;
参考文献
Mohamed, Yasser M.A.; Hansen, Trond Vidar
Tetrahedron, 2013 , vol. 69, # 19 p. 3872 - 3877
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; 1 h;
参考文献
Barrett, Anthony G. M.; Doubleday, Wendel W.; Tustin, Gary J.
Tetrahedron, 1996 , vol. 52, # 48 p. 15325 - 15338
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=25°C; Reduction; 0.5 h;
参考文献
Vinczer, Peter; Novak, Lajos; Szantay, Csaba
Organic Preparations and Procedures International, 1992 , vol. 24, # 3 p. 349 - 351
反应条件
1: With n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane T=0°C; 0.333333 h; 2: With (MeO)2BF in tetrahydrofuran; hexane T=-75°C; 3: With dihydrogen peroxide Alkaline hydrolysis; Title compound not separated from byproducts;
参考文献
Synthesis, , # 12 p. 1830 - 1836
反应条件
TfN(AlMe2)2 in dichloromethane
参考文献
Tetrahedron, , vol. 60, # 52 p. 12239 - 12247
反应条件
1: DMAP, DCC / CH2Cl2 / -20 - 20 °C 2: 1.) Ph3P, 2.) Dibal / 1) toluene, 50 deg C, 5 h; 2) toluene, 0 deg C, 30 min View Scheme
参考文献
Tetrahedron, , vol. 54, # 8 p. 1491 - 1496
反应条件
1: 95 percent / Aliquat 336 / 6 h / Heating 2: 95 percent / Red-Al / toluene / 0.5 h / 25 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 24, # 3 p. 349 - 351
反应条件
sodium tetrahydroborate in water 2 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Agricultural and Biological Chemistry, , vol. 46, # 7 p. 1757 - 1760
