(2E,4E)-2,4-己二烯-1-醇合成路线 （共 34 条）
反应条件
diisobutylaluminium hydride; triphenylphosphine 1) toluene, 50 deg C, 5 h; 2) toluene, 0 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 54, # 8 p. 1491 - 1496
反应条件
lithium aluminium tetrahydride Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 31, # 45 p. 6585 - 6588
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 2754,2759
反应条件
lithium aluminium tetrahydride
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 5 p. 1035 - 1040
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1146 - 1151
反应条件
mit UV-Licht.Irradiation;
参考文献
Chemische Berichte, , vol. 88, p. 1185,1194
反应条件
1: PBr3 / petroleum ether / -20 °C 2: 73 percent / 4 h / 150 - 160 °C 3: 1) n-BuLi, / 1) hexane, THF, 1 h, 0 deg C, 2) 30 min, -60 deg C; 12 h, r.t. 4: LiAlH4 / diethyl ether / 1) 1 h, 0 deg C, 2) 1 h, r.t. 5: 48 percent / p-toluenesulphonic acid / methanol; H2O / 2 h / 60 °C 6: pyridine View Scheme
参考文献
Bestmann, Hans Juergen; Koschatzky, Karl-Heinrich; Plenchette, Alain; Suess, Joachim; Vostrowsky, Otto
Liebigs Annalen der Chemie, 1982 , # 3 p. 536 - 544
反应条件
hydrogen; [Ru(C5Me5)(1,3-COD)]BF4 in acetone T=70°C; P=3750.38 Torr; Product distribution / selectivity;
参考文献
INNOVAROMA SA
Patent: WO2008/120174 A1, 2008 ;
Location in patent: Page/Page column 7; 9 ;
反应条件
hydrogen; [Ru(C5Me5)(1,3-COD)]BF4 in acetone T=70°C; P=3750.38 Torr; Product distribution / selectivity;
参考文献
INNOVAROMA SA
Patent: WO2008/120174 A1, 2008 ;
Location in patent: Page/Page column 7; 9 ;
反应条件
hydrogen; hexacarbonyl chromium in hexane T=160 - 180°C; P=38000 - 60800 Torr; 4 h;
参考文献
Steines, Stephan; Englert, Ulli; Driessen-Hoelscher, Birgit
Chemical Communications, 2000 , # 3 p. 217 - 218
反应条件
ammonium chloride in methanol Electrochemical reaction;
参考文献
Santana, Diogo S.; Lima, Marcio V. F.; Daniel, Jorge R. R.; Navarro, Marcelo
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4725 - 4727
