(2E,4E)-2,4-己二烯-1-醇合成路线 （共 34 条）
反应条件
ammonium chloride in methanol
Electrochemical reaction;
参考文献
Santana, Diogo S.; Lima, Marcio V. F.; Daniel, Jorge R. R.; Navarro, Marcelo
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4725 - 4727
反应条件
copper(l) iodide in tetrahydrofuran
参考文献
Tanigawa,Y. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 2361 - 2363
反应条件
1.1: CaH2; PBr3 / diethyl ether / 1.5 h / -5 - 23 °C
2.1: NaH / tetrahydrofuran / 0.25 h / -5 °C
2.2: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -5 °C
2.3: 48 percent / tetrahydrofuran; hexane / 0.33 h
View Scheme
参考文献
Ziegler, Frederick; Petersen, Anders K.
Journal of Organic Chemistry, 1994 , vol. 59, # 10 p. 2707 - 2714
反应条件
1.1: CaH2; PBr3 / diethyl ether / 1.5 h / -5 - 23 °C
2.1: NaH / tetrahydrofuran / 0.25 h / -5 °C
2.2: n-BuLi / tetrahydrofuran; hexane / 0.17 h / -5 °C
2.3: 48 percent / tetrahydrofuran; hexane / 0.33 h
3.1: 89 percent / triethylamine; para-acetamidobenzenesulfonyl azide / acetonitrile / 0.5 h / 23 °C
View Scheme
参考文献
Ziegler, Frederick; Petersen, Anders K.
Journal of Organic Chemistry, 1994 , vol. 59, # 10 p. 2707 - 2714
