(betaR)-beta-氨基-gamma-苯基-苯丙醇合成路线 (共 6 条)
反应条件
hydrogenchloride in tetrahydrofuran T=20°C; Hydrolysis; 24 h;
参考文献
Kanemasa; Adachi; Yamamoto; Wada
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 3 p. 681 - 687
反应条件
trifluorormethanesulfonic acid
参考文献
Klumpp; Aguirre; Sanchez Jr.; de Leon
Organic letters, 2001 , vol. 3, # 17 p. 2781 - 2784
反应条件
sodium hydroxide; hydrogen; palladium dihydroxide 1.) HCOOH, 60 deg C, 5 bar, 5 h; 2.) MeOH/H2O, reflux, 12 h; Yield given. Multistep reaction;
参考文献
Nunez, Marta G.; Farley, Alistair J. M.; Dixon, Darren J.
Journal of the American Chemical Society, 2013 , vol. 135, # 44 p. 16348 - 16351
反应条件
1: 77 percent / H2O2, LiOH / tetrahydrofuran; H2O / 3 h / Ambient temperature 2: 1.) triethylamine, (PhO)2P(O)N3, 2.) Ba(OH)2*8H2O / 1.) toluene, 80 deg C, 8 h, 2.) dioxane, water, reflux, 8 h View Scheme
参考文献
Takacs; Jaber; Vellekoop
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2742 - 2748
反应条件
barium dihydroxide; diphenyl phosphoryl azide; triethylamine 1.) toluene, 80 deg C, 8 h, 2.) dioxane, water, reflux, 8 h; Yield given. Multistep reaction;
参考文献
Takacs; Jaber; Vellekoop
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2742 - 2748
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in ethyl acetate 2 h;
参考文献
Koskinen, Ari M. P.; Hassila, Heikki; Myllymaeki, Vesa T.; Rissanen, Karl
Tetrahedron Letters, 1995 , vol. 36, # 31 p. 5619 - 5622