4-叔丁基杯[4]芳烃-冠-4-复合体合成路线 （共 10 条）
反应条件
1: p-tert-butyl calix[4]arene With sodium hydride in tetrahydrofuran; toluene; mineral oil
0.5 h; Reflux;
2: triethylene glycol di-p-tosylate in tetrahydrofuran; toluene; mineral oil
12 h; Reflux;
参考文献
Chawla, Har Mohindra; Hundal, Geeta; Kumar; Singh, Parminder
Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2012 , vol. 72, # 3-4 p. 323 - 330
反应条件
potassium carbonate; potassium iodide in acetonitrile
48 h; Heating;
参考文献
Gruen, Alajos; Koszegi, Eva; Bitter, Istvan
Tetrahedron, 2004 , vol. 60, # 23 p. 5041 - 5048
反应条件
potassium carbonate in acetonitrile
12 h;
参考文献
Alekseeva, Elena A.; Basok, Stepan S.; Mazepa, Alexander V.; Gren, Andrei I.
Mendeleev Communications, 2007 , vol. 17, # 6 p. 330 - 331
反应条件
potassium carbonate in acetonitrile
20 h;
参考文献
Alekseeva, Elena A.; Basok, Stepan S.; Mazepa, Alexander V.; Gren, Andrei I.
Mendeleev Communications, 2007 , vol. 17, # 6 p. 330 - 331
反应条件
potassium carbonate in acetonitrile
20 h;
参考文献
Alekseeva, Elena A.; Basok, Stepan S.; Mazepa, Alexander V.; Gren, Andrei I.
Mendeleev Communications, 2007 , vol. 17, # 6 p. 330 - 331
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene
T=20°C; Mitsunobu reaction; 0.5 h;
参考文献
Csokai, Viktor; Gruen, Alajos; Bitter, Istvan
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4681 - 4684
反应条件
potassium carbonate in acetonitrile
12 h;
参考文献
Alekseeva, Elena A.; Basok, Stepan S.; Mazepa, Alexander V.; Gren, Andrei I.
Mendeleev Communications, 2007 , vol. 17, # 6 p. 330 - 331
反应条件
potassium carbonate in acetonitrile
14 h;
参考文献
Alekseeva, Elena A.; Basok, Stepan S.; Mazepa, Alexander V.; Gren, Andrei I.
Mendeleev Communications, 2007 , vol. 17, # 6 p. 330 - 331
反应条件
1: 43 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 2 h / 20 °C
2: 55 percent / K2CO3; KI / acetonitrile / 48 h / Heating
View Scheme
参考文献
Gruen, Alajos; Koszegi, Eva; Bitter, Istvan
Tetrahedron, 2004 , vol. 60, # 23 p. 5041 - 5048
反应条件
1: 43 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 2 h / 20 °C
2: 55 percent / K2CO3; KI / acetonitrile / 48 h / Heating
View Scheme
参考文献
Gruen, Alajos; Koszegi, Eva; Bitter, Istvan
Tetrahedron, 2004 , vol. 60, # 23 p. 5041 - 5048
