montmorillonite K-10 in dichloromethane 0.133333 h; Irradiation;

<b>Multi-step reaction with 3 steps<br /> </b>1: NaH / tetrahydrofuran<br />2: LiAlH₄ / diethyl ether / 2 h / -50 &deg;C<br />3: 69 percent / Hg(OAc)2 / 170 - 175 &deg;C / in sealed tube<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '506071', constants.ctx, '0')">propionic acid</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=160&deg;C;&nbsp;48&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11324583', constants.ctx, '0')">1,1'-bis-(diphenylphosphino)ferrocene</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '11592550', constants.ctx, '0')">[RhCl(η²:η²-cycloocta-1,5-diene)]2</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605264', constants.ctx, '0')">1,2-dichloro-ethane</a> <br />T=40&deg;C;&nbsp;5&nbsp;h;&nbsp;&nbsp;Schlenk techniqueInert atmosphere;&nbsp;&nbsp;regioselective reaction;&nbsp;<br /> &nbsp;