反应条件
1.1: 100 percent / aq. NaOH / diethyl ether / 0 °C
2.1: LDA / tetrahydrofuran; hexane / 0.33 h / -10 °C
2.2: 65 percent / tetrahydrofuran; hexane / 1 h / -78 °C
3.1: Br2; AcOH / 3 h / 80 °C
4.1: 59 percent / dimethylformamide / 14 h / 20 °C
5.1: 74 percent / m-chloroperbenzoic acid / dimethylformamide / 14 h / 20 °C
View Scheme
参考文献
Miwatashi, Seiji; Arikawa, Yasuyoshi; Naruo, Ken-Ichi; Igaki, Keiko; Watanabe, Yasumasa; Kimura, Hiroyuki; Kawamoto, Tomohiro; Ohkawa, Shigenori
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 4 p. 410 - 418
