反应条件
1: 78 percent / triethylamine, N,N-dimethylaminopyridine / CH2Cl2 / 1 h / 0 °C
2: 1.) NaH, 2.) NaOH
3: 75 percent / aq. sodium chloride / dimethylformamide / 3 h / Heating
4: 1.) BH3*THF, 2.) HCl / 1.) reflux, 1 h, 2.) MeOH, reflux, 1 h
View Scheme
参考文献
Galeazzi, Roberta; Geremia, Silvano; Mobbili, Giovanna; Orena, Mario
Tetrahedron Asymmetry, 1996 , vol. 7, # 1 p. 79 - 88
