二甲基2,3-戊二烯二酸酯合成路线 (共 13 条)
反应条件
1: T=20°C; Cycloaddition; 1 h;
2: With triethylamine hydrofluoric acid in ethanol
Aromatisation; desilylation; elimination;
参考文献
Hussain, Ibrar; Yawer, Mirza A.; Appel, Bettina; Sher, Muhammad; Mahal, Ahmed; Villinger, Alexander; Fischer, Christine; Langer, Peter
Tetrahedron, 2008 , vol. 64, # 34 p. 8003 - 8009
反应条件
triethylamine hydrofluoric acid
1) 23 deg C, 20 min, 2) 95percent EtOH, 23 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Roush, William R.; Murphy, Megan
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6622 - 6629
反应条件
Cu(I)-tert-butoxide in tetrahydrofuran
T=-78°C;
参考文献
Bryson,T.A. et al.
Tetrahedron Letters, 1977 , p. 525 - 528