N-(2,5-二氯苯基)-2-(羟基亚氨基)乙酰胺合成路线 （共 4 条）
反应条件
hydroxylamine hydrochloride; sodium sulfate in ethanol; water T=80°C; 12 h; Inert atmosphereSchlenk technique;
参考文献
Chang, Ning-Hui; Chen, Xi-Chao; Nonobe, Hikaru; Okuda, Yasuhiro; Mori, Hiroki; Nakajima, Kiyohiko; Nishihara, Yasushi
Organic Letters, 2013 , vol. 15, # 14 p. 3558 - 3561
反应条件
1: KHCO3 / CH2Cl2 / -10 - 20 °C 2: hydroxylamine hydrochloride / ethanol; H2O / 2 h / Heating View Scheme
参考文献
Rewcastle, Gordon W.; Sutherland, Hamish S.; Weir, Claudette A.; Blackburn, Adrian G.; Denny, William A.
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8719 - 8721
反应条件
1: sulfuric acid / water / 0.25 h / 100 °C / |Inert atmosphere; |Schlenk technique 2: sodium hydroxide; dihydrogen peroxide / water / 0.5 h / 50 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Chang, Ning-Hui; Chen, Xi-Chao; Nonobe, Hikaru; Okuda, Yasuhiro; Mori, Hiroki; Nakajima, Kiyohiko; Nishihara, Yasushi
Organic Letters, 2013 , vol. 15, # 14 p. 3558 - 3561
反应条件
sulfuric acid in water T=100°C; 0.25 h; Inert atmosphereSchlenk technique;
参考文献
Chang, Ning-Hui; Chen, Xi-Chao; Nonobe, Hikaru; Okuda, Yasuhiro; Mori, Hiroki; Nakajima, Kiyohiko; Nishihara, Yasushi
Organic Letters, 2013 , vol. 15, # 14 p. 3558 - 3561
