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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
17122-60-0
合成路线
（共 5 条）
17122-60-0
→
反应条件
606-18-8
2-氨基-3-硝基苯甲酸
反应条件
1: sulfuric acid / 2.5 h / 90 °C / |Inert atmosphere 2: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
17122-60-0
→
反应条件
6924-71-6
喹噁啉-5-羧酸甲酯
反应条件
1: sulfuric acid / 2.5 h / 90 °C / |Inert atmosphere 2: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / |Inert atmosphere 3: hydrogenchloride / water / 12 h / |Reflux; |Inert atmosphere 4: palladium 10 on activated carbon; hydrogen / methanol / 8 h / |Inert atmosphere 5: water / 0.75 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
17122-60-0
→
反应条件
57113-91-4
2-氨基-3-硝基苯甲酸甲酯
反应条件
1: sulfuric acid / 2.5 h / 90 °C / |Inert atmosphere 2: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / |Inert atmosphere 3: hydrogenchloride / water / 12 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
17122-60-0
→
反应条件
112656-95-8
7-硝基靛红
反应条件
sulfuric acid T=90°C; 2.5 h; Inert atmosphere;
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
17122-60-0
→
反应条件
107582-20-7
2,3-二氨基苯甲酸甲酯
反应条件
1: sulfuric acid / 2.5 h / 90 °C / |Inert atmosphere 2: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / |Inert atmosphere 3: hydrogenchloride / water / 12 h / |Reflux; |Inert atmosphere 4: palladium 10 on activated carbon; hydrogen / methanol / 8 h / |Inert atmosphere View Scheme
参考文献
Wang, Jingjing; Zuo, Sujing; Chen, Weiqiang; Zhang, Xinrui; Tan, Kaixin; Tian, Yun; Wang, Jianhui
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8217 - 8231
