2-甲基-1,5-己二烯-3-醇合成路线 （共 10 条）
反应条件
in diethyl ether
T=35°C;
参考文献
Crimmins, Michael T.; Ellis, J. Michael; Emmitte, Kyle A.; Haile, Pamela A.; McDougall, Patrick J.; Parrish, Jonathan D.; Zuccarello, J. Lucas
Chemistry - A European Journal, 2009 , vol. 15, # 36 p. 9223 - 9234
参考文献
Viola,A. et al.
Journal of the American Chemical Society, 1967 , vol. 89, p. 3462 - 3470
反应条件
tetrabutylammonium trifluoromethanesulphonate in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Short, Joanne D.; Attenoux, Sandrine; Berrisford, David J.
Tetrahedron Letters, 1997 , vol. 38, # 13 p. 2351 - 2354
反应条件
acetic acid; mercury; zinc
参考文献
Mistryukov, E. A.; Korshevits, I. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 11 p. 2396 - 2397
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 11 p. 2612 - 2613
反应条件
acetic acid; allyl bromide; mercury; zinc
further reagents;
参考文献
Mistryukov, E. A.; Korshevits, I. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 11 p. 2396 - 2397
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 11 p. 2612 - 2613
参考文献
Mistryukov, E. A.; Korshevits, I. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 11 p. 2396 - 2397
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 11 p. 2612 - 2613
反应条件
ammonium chloride; magnesium
1.) THF, boiling, 7 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Akhmedov, M. A.; Akhmedov, I. M.; Mustafaeva, Z. G.; Sardarov, I. K.; Kostikov, R. R.; Musaeva, Kh. E.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 6.1 p. 1087 - 1088
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 6 p. 1257 - 1258
反应条件
ammonium chloride
1.) 25 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Boaretto, Andrea; Marton, Daniele; Silvestri, Rosanna; Tagliavini, Giuseppe
Gazzetta Chimica Italiana, 1985 , vol. 115, # 7 p. 391 - 392
反应条件
(i) Mg, (ii) /BRN= 1209258/; Multistep reaction;
参考文献
Gibson,T.W.; Erman,W.F.
Journal of Organic Chemistry, 1972 , vol. 37, # 8 p. 1148 - 1154
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; methyltriphenoxy-phosphonium iodide
参考文献
Spangler,C.W.; Hartford,T.W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1792 - 1796
