反应条件
1: 14 percent / Me3NO, pyridine, H2O, OsO4 / 2-methyl-propan-2-ol / 48 h / Heating 2: 93 percent / pyridine / CH2Cl2 / 1 h / 0 °C 3: 60 percent / NaN3, benzo-15-crown-5 / dimethylformamide / Ambient temperature 4: 90 percent / pyridine / CH2Cl2 / 0.17 h / 0 °C 5: 80 percent / tetrahydrofuran / 1 h / Ambient temperature 6: 91 percent / K2CO3 / methanol / 2 h / Ambient temperature 7: 80 percent / H2 / 20percent Pd(OH)2 on charcoal / ethanol View Scheme
参考文献
Shing, Tony K. M.; Wan, Leong H.
Journal of Organic Chemistry, 1996 , vol. 61, # 24 p. 8468 - 8479