4-甲氧基苯硼酸频那醇酯合成路线 （共 109 条）
反应条件
1: 2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane With potassium tert-butylate in 1,4-dioxane
0.166667 h; Inert atmosphereGlove box;
2: With IMesCuOtBu in 1,4-dioxane
T=20°C; 0.166667 h; Inert atmosphereGlove box;
3: (E)-1-(3-chloroprop-1-en-1-yl)-4-methoxybenzene in 1,4-dioxane
T=45°C; 24 h; Inert atmosphereGlove box; regioselective reaction;
参考文献
Whittaker, Aaron M.; Rucker, Richard P.; Lalic, Gojko
Organic Letters, 2010 , vol. 12, # 14 p. 3216 - 3218
反应条件
potassium carbonate in water; isopropyl alcohol
Suzuki-Miyaura Coupling; 3 h; Green chemistry;
参考文献
Pandarus, Valerica; Gingras, Genevieve; Beland, Francois; Ciriminna, Rosaria; Pagliaro, Mario
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 897 - 901
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water
T=100°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
反应条件
Pd-PEPPSI-IPent; potassium hydroxide in tetrahydrofuran
T=70°C; Suzuki-Miyaura Coupling; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Farmer, Jennifer L.; Hunter, Howard N.; Organ, Michael G.
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17470 - 17473
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20°C; Suzuki-Miyaura cross-coupling; 74 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
反应条件
1: potassium phosphate / tetrahydrofuran
2: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
反应条件
copper ferrite in dimethyl sulfoxide
T=100°C; 16 h; Green chemistry;
参考文献
Kundu, Debasish; Mukherjee, Nirmalya; Ranu, Brindaban C.
RSC Advances, 2013 , vol. 3, # 1 p. 117 - 125
反应条件
sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in ethanol; benzene
Suzuki-Miyaura cross-coupling; 11 h; Heating;
参考文献
Banwel, Martin G.; Sydnes, Magne O.
Australian Journal of Chemistry, 2004 , vol. 57, # 6 p. 537 - 548
