4-甲氧基苯硼酸频那醇酯合成路线 (共 109 条)
反应条件
triethylamine; bis(diphosphaferrocene)PdCl2 dimer in 1,4-dioxane T=80°C; 144 h;
参考文献
Melaimi, Mohand; Thoumazet, Claire; Ricard, Louis; Le Floch, Pascal
Journal of Organometallic Chemistry, 2004 , vol. 689, # 19 p. 2988 - 2994
反应条件
triethylamine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=100°C; 6 h;
参考文献
Murata, Miki; Sambommatsu, Tomoko; Watanabe, Shinji; Masuda, Yuzuru
Synlett, 2006 , # 12 p. 1867 - 1870
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2 h; Inert atmosphere; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane T=-78 - 20°C; 12 h; Inert atmosphere;
参考文献
Jo, Mi Young; Lim, Younhee; Ahn, Byung-Hyun; Lee, Gun Dae; Kim, Joo Hyun
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 2 p. 492 - 498
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran T=25°C; 24 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 127, # 30 p. 10539 - 10544
反应条件
triethylamine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane T=120°C; 24 h;
参考文献
Murata, Miki; Sambommatsu, Tomoko; Watanabe, Shinji; Masuda, Yuzuru
Synlett, 2006 , # 12 p. 1867 - 1870
反应条件
toluene-4-sulfonic acid in benzene 16 h; Heating;
参考文献
Banwel, Martin G.; Sydnes, Magne O.
Australian Journal of Chemistry, 2004 , vol. 57, # 6 p. 537 - 548
反应条件
triethylamine; dichloro bis(acetonitrile) palladium(II) T=110°C; 24 h;
参考文献
Billingsley, Kelvin L.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5589 - 5591
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran byproducts: KI, CH3OC6H5; react. of (B(OC(CH3)2)2)2 (1.5 equiv.), 4-MeOC6H4I (1 equiv.), CuI (10 molpercent), nBu3P (13 molpercent) and KOtBu (1.5 equiv.) at room temp.;
参考文献
Kleeberg, Christian; Dang, Li; Lin, Zhenyang; Marder, Todd B.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 5350 - 5354
Angewandte Chemie, 2009 , vol. 121, p. 5454 - 5458
反应条件
boron trifluoride diethyl etherate in acetonitrile T=0°C; 0.0833333 h; Inert atmosphere;
参考文献
Zhu, Chuan; Yamane, Motoki
Organic Letters, 2012 , vol. 14, # 17 p. 4560 - 4563
反应条件
potassium acetate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane T=80°C; 2 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Miyaura, Norio
Tetrahedron, 2001 , vol. 57, # 49 p. 9813 - 9816