4-甲氧基苯硼酸频那醇酯合成路线 （共 109 条）
反应条件
catalyst: Pd#1,1'-bis(diphenylphosphino)ferrocene; triethylamine; CH3OH in diethyl ether byproducts: CH3OC6H5; 1. BH2N(CH(CH3)2)2, CH3OC6H4Br, (Pd), (C2H5)3N, toluene, 100°C, 1h; 2. CH3OH, room temp., 1 h; 3. pinacol, (C2H5)2O, room temp., 4 h;
参考文献
Gendrineau, Thomas; Marre, Samuel; Vaultier, Michel; Pucheault, Mathieu; Aymonier, Cyril
Angewandte Chemie - International Edition, 2012 , vol. 51, # 34 p. 8525 - 8528
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 13 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
反应条件
potassium acetate; palladium diacetate in benzene T=60°C; 10 h; Inert atmosphere;
参考文献
Kawamorita, Soichiro; Ohmiya, Hirohisa; Iwai, Tomohiro; Sawamura, Masaya
Angewandte Chemie - International Edition, 2011 , vol. 50, # 36 p. 8363 - 8366
反应条件
NaOC(CH3)3; 2,4,6-(i-Pr)3C6H2C6H4[2-P(cyclo-C6H11)2]; KOAc in ethanol mixt. org. compound, B2(OH)4, Pd-complex, (iPr)3C6H2C6H4-2-P(cyclo-C6H11), NaOBu-t and excess KOAc in EtOH at 80°C for 18 h;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Dreher, Spencer D.
Journal of the American Chemical Society, 2010 , vol. 132, # 50 p. 17701 - 17703
反应条件
potassium acetate; palladium diacetate in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
反应条件
potassium tetrachloropalladate; potassium acetate T=70°C; Miyaura borylation; 1.5 h; Inert atmosphere;
参考文献
Bej, Ansuman; Srimani, Dipankar; Sarkar, Amitabha
Green Chemistry, 2012 , vol. 14, # 3 p. 661 - 667
反应条件
1,2-bis(dimethylphosphine)ethane; (η5-indenyl)Ir(cod) T=150°C; 3 h; sealed tube; regioselective reaction;
参考文献
Chemical Communications, , vol. 46, # 41 p. 7724 - 7726
反应条件
[Ir(OMe)(1,5-cyclooctadiene)]2 in benzene T=80°C; 12 h; Schlenk techniqueInert atmosphere; Overall yield = 88 percent; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 136, # 10 p. 4003 - 4011
反应条件
N-bromosuccinimide; PdCl2(dppf); KOAc; Gold (III) chloride in dimethylsulfoxide; 1,2-dichloro-ethane 80°C;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 11 p. 2028 - 2032
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: para-iodoanisole in ethylene glycol dimethyl ether T=30°C; 1 h;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
