4-甲氧基苯硼酸频那醇酯合成路线 (共 109 条)
反应条件
1: triethylamine; 1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride / 1,4-dioxane / 6 h / 80 °C / |Sealed tube 2: hydrogenchloride / water / 15 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 88, # 1 p. 193 - 199
反应条件
in tetrahydrofuran T=25°C; 1 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 23 p. 9602 - 9610
反应条件
1: in toluene T=0 - 20°C; 2: in toluene T=50°C;
参考文献
Organic Process Research and Development, , vol. 12, # 6 p. 1265 - 1268
反应条件
iridium(hydrotris(pyrazolyl)borate)(1,5-cyclooctadiene) T=120°C; 16 h; Title compound not separated from byproducts.;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 79, # 12 p. 1980 - 1982
反应条件
1: methanol / 1 h / 0 - 20 °C / |Inert atmosphere 2: diethyl ether / 4 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 55, # 10 p. 1702 - 1705
反应条件
potassium phosphate in tetrahydrofuran Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 77, # 14 p. 5956 - 5964
反应条件
potassium fluoride in N,N-dimethyl-formamide T=50°C; 18 h; Inert atmosphere;
参考文献
Litvinas, Nichole D.; Fier, Patrick S.; Hartwig, John F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 536 - 539
反应条件
1-fluoro-2,4,6-trimethylpyridinium hexafluorophosphate; C10H18CuN2(1+)*CF3O3S(1-); silver fluoride in tetrahydrofuran T=50°C; 18 h; Inert atmosphere;
参考文献
Fier, Patrick S.; Luo, Jingwei; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 7 p. 2552 - 2559
反应条件
potassium phosphate in tetrahydrofuran Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 77, # 14 p. 5956 - 5964
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene 48 h; Heating / reflux;
参考文献
Koninklijke Philips Electronics N.V.
Patent: EP1838671 B1, 2008 ;
Location in patent: Page/Page column 11 ;