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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-乙酰苯基硼酸,醇酯
合成路线
（共 38 条）
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
3233-32-7
4-乙酰氧基苯酚
+
123-31-9
对苯二酚
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; 8 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
3233-32-7
4-乙酰氧基苯酚
+
99-93-4
对羟基苯乙酮
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca, M446G mutant; NADPH in dimethyl sulfoxide T=30°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
20062-24-2
p-叠氮基苯乙酮
反应条件
trimethylsilylazide; tetrabutyl ammonium fluoride; copper(l) chloride in tetrahydrofuran; methanol 7.5 h; RefluxIn air;
参考文献
Li, Yu; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 7969 - 7972
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
99-93-4
对羟基苯乙酮
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca; NADPH in dimethyl sulfoxide T=30°C; 1 h; Tris/HCl bufferEnzymatic reaction; chemoselective reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
3233-32-7
4-乙酰氧基苯酚
+
99-93-4
对羟基苯乙酮
反应条件
phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca, M446G mutant; NADPH in dimethyl sulfoxide T=30°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
403-42-9
4-氟苯乙酮
+
455-36-7
3'-氟苯乙酮
反应条件
AcOF in acetic acid; acetonitrile T=0 - 20°C; 0.333333 h;
参考文献
Vints, Inna; Gatenyo, Julia; Rozen, Shlomo
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11794 - 11797
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
403-42-9
4-氟苯乙酮
反应条件
1-fluoro-2,4,6-trimethylpyridinium hexafluorophosphate; C10H18CuN2(1+)*CF3O3S(1-); silver fluoride in tetrahydrofuran T=50°C; 18 h; Inert atmosphere;
参考文献
Fier, Patrick S.; Luo, Jingwei; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 7 p. 2552 - 2559
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
123-31-9
对苯二酚
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
3233-32-7
4-乙酰氧基苯酚
+
123-31-9
对苯二酚
反应条件
4-hydroxyacetophenone monooxygenase from Pseudomonas fluorescens; phosphite dehydrogenase; NADPH in dimethyl sulfoxide T=24°C; 8 h; Tris/HCl bufferEnzymatic reaction;
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
100-44-7
苄基氯
+
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
782-92-3
4-(乙酰苯基)苯甲烷
反应条件
potassium tetrachloropalladate; cesium fluoride T=70°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Bej, Ansuman; Srimani, Dipankar; Sarkar, Amitabha
Green Chemistry, 2012 , vol. 14, # 3 p. 661 - 667
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