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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-溴芘
合成路线
（共 88 条）
1714-29-0
1-溴芘
→
反应条件
188-90-9
反应条件
aluminium trichloride T=140°C;
参考文献
Ammerer; Zinke
Monatshefte fuer Chemie, 1953 , vol. 84, p. 25,30
1714-29-0
1-溴芘
→
反应条件
196-28-1
二苯并(c,mno)屈
反应条件
1: CsF / Pd(PPh3)4 / 1,2-dimethoxy-ethane / 15 h / Heating 2: aq. KOH / acetonitrile / 16 h / 65 - 70 °C 3: MeSO3H / CH2Cl2 / 15 h / 20 °C View Scheme
参考文献
Kumar, Subodh
Synthesis, 2001 , # 6 p. 841 - 844
75-77-4
三甲基氯硅烷
+
1714-29-0
1-溴芘
→
反应条件
18662-97-0
反应条件
1: 1-Bromopyrene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere;
参考文献
Niko, Yosuke; Kawauchi, Susumu; Otsu, Shun; Tokumaru, Katsumi; Konishi, Gen-Ichi
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3196 - 3207
1013-88-3
+
1714-29-0
1-溴芘
→
反应条件
30269-02-4
+
30269-01-3
反应条件
1: 1-Bromopyrene With nitric acid; acetic acid T=20°C; Nitration; 24 h; 2: N-(diphenylmethylene)amine With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; palladium diacetate in tetrahydrofuran Condensation; 16 h; Heating; 3: With hydrogenchloride in tetrahydrofuran T=20°C; Hydrolysis; 0.0833333 h; Further stages.;
参考文献
Purohit, Vandana; Basu, Ashis K.
Organic Letters, 2000 , vol. 2, # 13 p. 1871 - 1874
1714-29-0
1-溴芘
+
536-74-3
→
反应条件
23975-18-0
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine 48 h; Reflux;
参考文献
Yamashita, Hiroaki; Abe, Jiro
Journal of Physical Chemistry A, 2011 , vol. 115, # 46 p. 13332 - 13337
1013-88-3
+
1714-29-0
1-溴芘
→
反应条件
30269-02-4
+
30269-01-3
反应条件
1: 1-Bromopyrene With nitric acid; acetic acid T=20°C; Nitration; 24 h; 2: N-(diphenylmethylene)amine With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; palladium diacetate in tetrahydrofuran Condensation; 16 h; Heating; 3: With hydrogenchloride in tetrahydrofuran T=20°C; Hydrolysis; 0.0833333 h; Further stages.;
参考文献
Purohit, Vandana; Basu, Ashis K.
Organic Letters, 2000 , vol. 2, # 13 p. 1871 - 1874
→
反应条件
3029-19-4
+
1448061-63-9
反应条件
1: 1-Bromopyrene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2 h; 2: 2,5-dioctyldithieno[2,3-b:3’,2’-d]thiophene in tetrahydrofuran; hexane T=0°C; 3 h; 3: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=20°C;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 767 - 774
→
反应条件
3029-19-4
+
1448061-62-8
反应条件
1: 1-Bromopyrene With tert.-butyl lithium in tetrahydrofuran; hexane T=-78°C; 2 h; 2: 2,5-dioctyldithieno[2,3-b:3’,2’-d]thiophene in tetrahydrofuran; hexane T=0°C; 3 h; 3: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78°C;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 767 - 774
1714-29-0
1-溴芘
→
反应条件
781-17-9
反应条件
1: NaOMe / methanol / Irradiation 2: 70 percent / diethyl malonate, NaOEt / ethanol / 12 h / Irradiation View Scheme
参考文献
Recueil: Journal of the Royal Netherlands Chemical Society, , vol. 102, # 4 p. 224 - 228
1714-29-0
1-溴芘
→
反应条件
129-00-0
反应条件
triethylamine in methanol; water T=4°C; 0.25 h; Irradiationsensitizer: methylene blue;
参考文献
Venkatarangan, Lata; Yang, Dan-Hui; Epling, Gary A.; Basu, Ashis K.
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1441 - 1444
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