反应条件
hydrogenchloride; n-butyllithium in diethyl ether; hexane BuLi soln. (hexane) addn. to org. compd. soln. (Et2O) at 0°C, mixt. addn. to B-compd. soln. (Et2O) at -78°C over 30 min, stirring 3 h at -50 to -70°C and 60 h at room temp., 2 M HCl addn., stirring 2 h, org. phase sepn.; org. phase washing (water), drying (MgSO4), treating with charcoal, ethereal soln. concn. to dryness, residue vac. drying at 50°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1263 - 1268
