4-苯基-1,2-恶唑-5(2H)-酮合成路线 (共 2 条)
反应条件
manganese(IV) oxide; triethylamine
1) CH2Cl2, 15 min, room temperature, 2) reflux, 15 min; Multistep reaction;
参考文献
Beccalli, Egle M.; Rosa, Concetta La; Marchesini, Alessandro
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4287 - 4290
反应条件
1: 60 percent / POCl3 / CHCl3 / 2 h / Heating
2: 86 percent / NaOH, H2O / dioxane / 2 h / Ambient temperature
3: 25 mg / 10percent H2SO4 / dioxane / 2 h / Heating
View Scheme
参考文献
Beccalli, Egle M.; Marchesini, Alessandro
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3426 - 3434