N-苄基-N-(3-丁烯)胺合成路线 (共 24 条)
反应条件
1: pyridine / benzene / 20 °C 2: DMAP / CH2Cl2 / 20 °C 3: 1,1'-azo-bis-cyclohexane-1-carbonitrile / toluene / Heating View Scheme
参考文献
Jackson; Walton
Chemical Communications, 2000 , # 23 p. 2327 - 2328
参考文献
Tebben, Gerd-Dieter; Rauch, Karsten; Stratmann, Christian; Williams, Craig M.; De Meijere, Armin
Organic Letters, 2003 , vol. 5, # 4 p. 483 - 485
反应条件
1.1: 81 percent / Et3N / CH2Cl2 / 0 - 25 °C 2.1: O3 / methanol; CH2Cl2 / -78 °C 2.2: Me2S / CH2Cl2; methanol / 12 h / 20 °C View Scheme
参考文献
Aurrecoechea, Jose M.; Fernandez, Alvaro; Gorgojo, Jose M.; Saornil, Carlos
Tetrahedron, 1999 , vol. 55, # 23 p. 7345 - 7362
反应条件
1: 78 percent / Et3N / tetrahydrofuran / 15 h / Ambient temperature
2: 43 percent / 10percent Pd/C / toluene / 24 h / Heating
View Scheme
参考文献
Noguchi, Michihiko; Kakimoto, Shinji; Kawakami, Hisao; Kajigaeshi, Shoji
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 5 p. 1355 - 1362