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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氟三丁基甲锡烷基苯
合成路线
（共 35 条）
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
540-36-3
1,4-二氟苯
反应条件
sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Tang, Pingping; Furuya, Takeru; Ritter, Tobias
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 12150 - 12154
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
540-36-3
1,4-二氟苯
反应条件
water; sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Tang, Pingping; Furuya, Takeru; Ritter, Tobias
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 12150 - 12154
3582-05-6
三氟乙基三氟甲烷磺酸酯
+
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
67-56-1
甲醇
+
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
459-60-9
4-氟苯甲醚
+
540-36-3
1,4-二氟苯
反应条件
sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Tang, Pingping; Furuya, Takeru; Ritter, Tobias
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 12150 - 12154
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With silver nitrate; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
371-41-5
4-氟苯酚
+
540-36-3
1,4-二氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium trifluoro-methanesulfonate; tris(dimethylamino)sulfonium trifluoromethoxide in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With AgPF6; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
540-36-3
1,4-二氟苯
反应条件
water; sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Tang, Pingping; Furuya, Takeru; Ritter, Tobias
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 12150 - 12154
17151-47-2
4-氟三丁基甲锡烷基苯
+
96898-10-1
→
反应条件
462-06-6
氟苯
+
371-41-5
4-氟苯酚
+
352-67-0
4-三氟甲氧基氟苯
反应条件
1: With trifluoromethanesulfonic acid trifluoromethyl ester; sodium hydrogencarbonate in tetrahydrofuran T=-30°C; Inert atmosphere; 2: With silver nitrate; F-TEDA-PF6 in tetrahydrofuran; acetone T=-30 - 23°C; Inert atmosphereDarkness;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
540-36-3
1,4-二氟苯
反应条件
methanol; sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Tang, Pingping; Furuya, Takeru; Ritter, Tobias
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 12150 - 12154
17151-47-2
4-氟三丁基甲锡烷基苯
→
反应条件
462-06-6
氟苯
+
540-36-3
1,4-二氟苯
反应条件
sodium trifluoro-methanesulfonate; sodium hydrogencarbonate; F-TEDA-PF6; silver(l) oxide in acetone T=65°C; 5 h; Sealed vialInert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 34 p. 12150 - 12154
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