三丁基(4-氯苯基)锡烷合成路线 (共 30 条)
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
CuDPP in N,N-dimethyl-formamide
T=60°C; 12 h; Inert atmosphere;
参考文献
Zhang, Zhihui; Yu, Ying; Liebeskind, Lanny S.
Organic Letters, 2008 , vol. 10, # 14 p. 3005 - 3008
反应条件
iodobenzene dichloride; bis(benzonitrile)palladium(II) dichloride in diethyl ether
T=0 - 20°C; Heck reaction; 13 h;
参考文献
Kalyani, Dipannita; Satterfield, Andrew D.; Sanford, Melanie S.
Journal of the American Chemical Society, 2010 , vol. 132, # 24 p. 8419 - 8427
反应条件
bis(benzonitrile)palladium(II) dichloride; copper dichloride in diethyl ether
T=0 - 25°C; 12 h;
参考文献
Kalyani, Dipannita; Satterfield, Andrew D.; Sanford, Melanie S.
Journal of the American Chemical Society, 2010 , vol. 132, # 24 p. 8419 - 8427
反应条件
MCM-41-supported bidentate phosphine palladium(0) complex in N,N-dimethyl-formamide
T=80°C; Stille carbonylative cross-coupling; P=760.051 Torr; 6 h;
参考文献
Cai, Mingzhong; Zheng, Guomin; Ding, Guodong
Green Chemistry, 2009 , vol. 11, # 10 p. 1687 - 1693
反应条件
aluminium trichloride in dichloromethane
1.) 0 deg C, 2 h, 2.) r.t., 2 h;
参考文献
Arnswald, Martin; Neumann, Wilhelm P.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7022 - 7028
反应条件
palladium diacetate in tetrahydrofuran
T=20°C; Stille reaction; 1.5 h;
参考文献
Dughera, Stefano
Synthesis, 2006 , # 7 p. 1117 - 1122
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide
T=60°C; Stille coupling; 6 h;
参考文献
Zhao, Hong; Wang, Yue; Sha, Junchao; Sheng, Shouri; Cai, Mingzhong
Tetrahedron, 2008 , vol. 64, # 32 p. 7517 - 7523
反应条件
palladium diacetate in tetrahydrofuran
T=20°C; Stille reaction; 1.75 h;
参考文献
Dughera, Stefano
Synthesis, 2006 , # 7 p. 1117 - 1122
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide
T=60°C; Stille coupling; 8 h;
参考文献
Zhao, Hong; Wang, Yue; Sha, Junchao; Sheng, Shouri; Cai, Mingzhong
Tetrahedron, 2008 , vol. 64, # 32 p. 7517 - 7523