二苯基(三甲基硅基)膦合成路线 （共 101 条）
反应条件
1: triphenylphosphine in tetrahydrofuran T=20°C; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran 0.166667 h; Inert atmosphere;
参考文献
Nandi, Partha; Dye, James L.; Bentley, Philip; Jackson, James E.
Organic Letters, 2009 , vol. 11, # 8 p. 1688 - 1692
反应条件
1: chloro-diphenylphosphine With lithium in tetrahydrofuran T=20°C; 3 h; 2: chloro-trimethyl-silane in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Chemical Communications, , # 14 p. 1848 - 1850
反应条件
N'''-tert-butyl-N,N,N',N',N'',N''-hexamethylphosphorimidic triamide in tetrahydrofuran; diethyl ether 24 h; Ambient temperature;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 81, # 1-4 p. 155 - 164
反应条件
lithium 1.) THF, overnight, 2.) THF; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 52, # 5 p. 748 - 753
反应条件
P4 1.) toluol, -78 deg C, 2.) toluol, r.t.; Multistep reaction;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 22, p. 323 - 336
参考文献
Chemische Berichte, , vol. 92, p. 227,23000
参考文献
Chemische Berichte, , vol. 130, # 11 p. 1663 - 1670
反应条件
1: 89 percent / diethyl ether / 4 h / -80 °C 2: CHCl3 / 0.08 h / 20 - 35 °C View Scheme
参考文献
Lindner, Ekkehard; Merkle, Ralf Dieter; Hiller, Wolfgang; Fawzi, Riad
Chemische Berichte, 1986 , vol. 119, # 2 p. 659 - 668
反应条件
[NiCl2(PPh3)2]; potassium tert-butylate in 1,4-dioxane T=90°C; 10 h; Inert atmosphere;
参考文献
Sun, Meng; Zhang, Hong-Yu; Han, Qi; Yang, Kuo; Yang, Shang-Dong
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9566 - 9570
参考文献
Mont, Wolf-Walther du; Severengiz, Tevfik; Meyer, Bernd
Angewandte Chemie, 1983 , vol. 95, # 12 p. 1025 - 1026
