二苯基(三甲基硅基)膦合成路线 （共 101 条）
反应条件
silver trifluoromethanesulfonate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in methanol; benzene Heating;
参考文献
Hayashi, Minoru; Matsuura, Yutaka; Watanabe, Yutaka
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9248 - 9251
反应条件
dichloro bis(acetonitrile) palladium(II) T=100°C; 2 h; Title compound not separated from byproducts;
参考文献
Veits, Yu. A.; Karlstedt, N. B.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 1.1 p. 70 - 73
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 1 p. 66 - 69
反应条件
cesium fluoride in N,N-dimethyl-formamide T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Reis, Andreas; Dehe, Daniel; Farsadpour, Saeid; Munstein, Isabel; Sun; Thiel, Werner R.
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2488 - 2495
反应条件
1: 88.5 percent / petroleum ether / 0.5 h / -40 °C 2: 46.4 percent / O2 / diethyl ether / 20 °C 3: CHCl3 View Scheme
参考文献
Lindner, Ekkehard; Tamoutsidis, Efstathios
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 6 p. 726 - 732
反应条件
[NiCl2(PPh3)2]; potassium tert-butylate in 1,4-dioxane T=90°C; 10 h; Inert atmosphere;
参考文献
Sun, Meng; Zhang, Hong-Yu; Han, Qi; Yang, Kuo; Yang, Shang-Dong
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9566 - 9570
反应条件
in hexane T=-30 - 20°C; Inert atmosphere;
参考文献
Banger, Kulbinder K.; Brisdon, Alan K.; Herbert, Christopher J.; Ghaba, Hana Ali; Tidmarsh, Ian S.
Journal of Fluorine Chemistry, 2009 , vol. 130, # 12 p. 1117 - 1129
反应条件
B(C6F4H)3; heptane-4-one; bromobenzene-d5 T=130°C; 120 h; Inert atmosphereSchlenk technique; Concentration;
参考文献
Organometallics, , vol. 32, # 16 p. 4469 - 4472
反应条件
1: toluene 2: H2O / benzene View Scheme
参考文献
Polyhedron, , vol. 7, p. 2091 - 2094
反应条件
in benzene T=100°C; 2 h;
参考文献
Russian Journal of General Chemistry, , vol. 72, # 11 p. 1790 - 1792
反应条件
B(C6F4H)3; heptane-4-one; bromobenzene-d5 T=130°C; 120 h; Inert atmosphereSchlenk technique; Concentration;
参考文献
Organometallics, , vol. 32, # 16 p. 4469 - 4472
