二苯基(三甲基硅基)膦合成路线 (共 101 条)
参考文献
Mont, Wolf-Walther du; Severengiz, Tevfik; Meyer, Bernd
Angewandte Chemie, 1983 , vol. 95, # 12 p. 1025 - 1026
反应条件
in toluene T=25°C; 120 h;
参考文献
Burck, Sebastian; Foerster, Daniela; Gudat, Dietrich
Chemical Communications, 2006 , # 26 p. 2810 - 2812
反应条件
1,1'-azobis(cyclohexane)-1-carbonitrile in n-heptane T=100°C; 72 h;
参考文献
Vaillard, Santiago E.; Mueck-Lichtenfeld, Christian; Grimme, Stefan; Studer, Armido
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6533 - 6536
反应条件
1,1'-azobis(cyclohexane)-1-carbonitrile in n-heptane T=100°C; 72 h;
参考文献
Vaillard, Santiago E.; Mueck-Lichtenfeld, Christian; Grimme, Stefan; Studer, Armido
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6533 - 6536
反应条件
2-Cl-1,3-(2,6-Me2C6H3)2-2,3-dihydro-1H-[1,3,2]diazaphosphole in toluene T=50°C; 48 h;
参考文献
Burck, Sebastian; Foerster, Daniela; Gudat, Dietrich
Chemical Communications, 2006 , # 26 p. 2810 - 2812
反应条件
in dichloromethane T=-78 - 20°C;
参考文献
Eisenberger, Patrick; Kieltsch, Iris; Armanino, Nicolas; Togni, Antonio
Chemical Communications, 2008 , # 13 p. 1575 - 1577
反应条件
in hexane T=-30 - 20°C; Inert atmosphere;
参考文献
Banger, Kulbinder K.; Brisdon, Alan K.; Herbert, Christopher J.; Ghaba, Hana Ali; Tidmarsh, Ian S.
Journal of Fluorine Chemistry, 2009 , vol. 130, # 12 p. 1117 - 1129
反应条件
in dichloromethane-d2 T=20°C; 24 h;
参考文献
Eisenberger, Patrick; Kieltsch, Iris; Armanino, Nicolas; Togni, Antonio
Chemical Communications, 2008 , # 13 p. 1575 - 1577
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene T=60°C; 36 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
[NiCl2(PPh3)2]; potassium tert-butylate in 1,4-dioxane T=90°C; 10 h; Inert atmosphere;
参考文献
Sun, Meng; Zhang, Hong-Yu; Han, Qi; Yang, Kuo; Yang, Shang-Dong
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9566 - 9570