二苯基(三甲基硅基)膦合成路线 （共 101 条）
反应条件
T=10°C; Addition; 0.5 h;
参考文献
Kabachnik; Khomutova; Beletskaya
Russian Chemical Bulletin, 1999 , vol. 48, # 12 p. 2352 - 2353
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene
T=60°C; 28 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=20°C; 1 h; Inert atmosphere;
参考文献
Reis, Andreas; Dehe, Daniel; Farsadpour, Saeid; Munstein, Isabel; Sun; Thiel, Werner R.
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2488 - 2495
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene
T=60°C; 28 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=20°C; 0.833333 h; Inert atmosphere;
参考文献
Reis, Andreas; Dehe, Daniel; Farsadpour, Saeid; Munstein, Isabel; Sun; Thiel, Werner R.
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2488 - 2495
反应条件
cesium fluoride in N,N-dimethyl-formamide
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Reis, Andreas; Dehe, Daniel; Farsadpour, Saeid; Munstein, Isabel; Sun; Thiel, Werner R.
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2488 - 2495
反应条件
in toluene
T=25°C; 24 h;
参考文献
Burck, Sebastian; Foerster, Daniela; Gudat, Dietrich
Chemical Communications, 2006 , # 26 p. 2810 - 2812
参考文献
Fenske,D.; Becher,H.J.
Chemische Berichte, 1975 , vol. 108, p. 2115 - 2123
反应条件
2-Cl-1,3-(2,6-Me2C6H3)2-2,3-dihydro-1H-[1,3,2]diazaphosphole in toluene
T=90°C; 24 h;
参考文献
Burck, Sebastian; Foerster, Daniela; Gudat, Dietrich
Chemical Communications, 2006 , # 26 p. 2810 - 2812
反应条件
1: 79 percent / LiCl / tetrahydrofuran / -78 - 20 °C
2: CH2Cl2 / 12 h
View Scheme
参考文献
Reisser, Martin; Maier, Alexandra; Maas, Gerhard
European Journal of Organic Chemistry, 2003 , # 11 p. 2071 - 2079
