二苯基(三甲基硅基)膦合成路线 （共 101 条）
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene
T=50°C; 36 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
in benzene
72 h; Heating;
参考文献
Tasz, Maciej K.; Gamliel, Asher; Rodriguez, Oscar P.; Lane, Thomas M.; Cremer, Sheldon E.; Bennett, Dennis W.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6281 - 6288
反应条件
in diethyl ether
T=0°C; 1 h;
参考文献
Mao, Fei; Tyler, David R.; Keszler, Doug
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 130 - 134
反应条件
2-Cl-1,3-(2,6-Me2C6H3)2-2,3-dihydro-1H-[1,3,2]diazaphosphole in toluene
T=90°C; 170 h;
参考文献
Burck, Sebastian; Foerster, Daniela; Gudat, Dietrich
Chemical Communications, 2006 , # 26 p. 2810 - 2812
反应条件
in diethyl ether; toluene
addn. of equimolar amts. of Me3SiPPh2 in toluene to satd. soln. of (p-MePh)2(CH2CHPh)SnCl in ether, 1h, room temp., stirred, distn. under vac.,under Ar; elem. anal.;
参考文献
Schumann, H.; Rodewald, G.; Lefferts, J. L.; Zuckerman, J. J.
Journal of Organometallic Chemistry, 1980 , vol. 190, # 1 p. 53 - 64
反应条件
in Petroleum ether
0.5 h;
参考文献
Lindner, Ekkehard; Huebner, Dieter
Chemische Berichte, 1983 , vol. 116, # 7 p. 2574 - 2590
反应条件
in Petroleum ether
0.5 h;
参考文献
Lindner, Ekkehard; Huebner, Dieter
Chemische Berichte, 1983 , vol. 116, # 7 p. 2574 - 2590
反应条件
in Petroleum ether
0.5 h;
参考文献
Lindner, Ekkehard; Huebner, Dieter
Chemische Berichte, 1983 , vol. 116, # 7 p. 2574 - 2590
反应条件
in diethyl ether
-80 deg C to -20 deg C;
参考文献
Lindner, Ekkehard; Steinwand, Michael; Hoehne, Sigurd
Chemische Berichte, 1982 , vol. 115, # 6 p. 2181 - 2191
反应条件
in diethyl ether
-80 deg C to -20 deg C;
参考文献
Lindner, Ekkehard; Steinwand, Michael; Hoehne, Sigurd
Chemische Berichte, 1982 , vol. 115, # 6 p. 2181 - 2191
