9,9-二甲基-9-硅杂双环[4.3.0]壬-1,3,5-三烯合成路线 （共 6 条）
参考文献
Ando,W. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 6995 - 6999
反应条件
1.1: magnesium / tetrahydrofuran / |Inert atmosphere
1.2: 24 h / 25 °C / |Inert atmosphere
2.1: [RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,3-bis-(diphenylphosphino)propane / 1,4-dioxane / 4 h / 25 - 180 °C
View Scheme
参考文献
Kuninobu, Yoichiro; Nakahara, Takahiro; Takeshima, Hirotaka; Takai, Kazuhiko
Organic Letters, 2013 , vol. 15, # 2 p. 426 - 428
反应条件
T=500°C; Further byproducts given;
参考文献
Sekiguchi, Akira; Ando, Wataru
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5286 - 5290
反应条件
T=500°C; Further byproducts given;
参考文献
Sekiguchi, Akira; Ando, Wataru
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5286 - 5290
参考文献
Barton,J.; Juvet,M.
Tetrahedron Letters, 1975 , p. 3893 - 3896
反应条件
T=500°C; pyrolysis of var. 1-(trimethylsilyl)-1-alkanols; Product distribution;
参考文献
Sekiguchi, Akira; Ando, Wataru
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5286 - 5290
