2,2-二氟-2-(氟磺酰)醋酸盐合成路线 （共 68 条）
反应条件
sodium sulfate in acetonitrile
T=60°C; 2 h;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Organic Chemistry, 1989 , vol. 54, # 13 p. 3023 - 3027
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
反应条件
sodium chloride in water; acetonitrile
T=25°C; 5 h; catalyst NaCl; various amounts of catalyst and solvent; different temp. and reaction times;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Fluorine Chemistry, 1990 , vol. 47, # 3 p. 509 - 514
反应条件
hidrolization; isolation as salt by Ba(OH)2 or CaCO3;
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
in water
byproducts: SO2; heating, solvent: acid soln.;
参考文献
Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1499 - 1501
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1606 - 1610
C.A., 1962 , vol. 56, p. 7116
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
sodium sulfate in acetonitrile
T=50°C; 1 h;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Fluorine Chemistry, 1989 , vol. 44, p. 433 - 440
反应条件
copper(l) iodide in acetonitrile
T=50°C; 2 h;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Fluorine Chemistry, 1989 , vol. 44, p. 433 - 440
反应条件
sodium chloride in water; acetonitrile
T=25°C; 5 h; catalyst NaCl; various amounts of catalyst and solvent; different temp. and reaction times;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Fluorine Chemistry, 1990 , vol. 47, # 3 p. 509 - 514
