(2S,4S)-3-苄氧羰基-4-甲基-2-苯基-1,3-恶唑啉-5-酮合成路线 （共 6 条）
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=-15°C; 96 h;
参考文献
Long, Ya-Qiu; Xue, Ting; Song, Yan-Li; Liu, Zu-Long; Huang, Shao-Xu; Yu, Qiang
Journal of Medicinal Chemistry, 2008 , vol. 51, # 20 p. 6371 - 6380
反应条件
in dichloromethane
T=0 - 25°C;
参考文献
Long, Ya-Qiu; Xue, Ting; Song, Yan-Li; Liu, Zu-Long; Huang, Shao-Xu; Yu, Qiang
Journal of Medicinal Chemistry, 2008 , vol. 51, # 20 p. 6371 - 6380
反应条件
1: ZnCl2; SOCl2 / tetrahydrofuran-d8 / 20 °C
2: ZnCl2 / tetrahydrofuran
3: ZnCl2
View Scheme
参考文献
Eriksson, Magnus; Napolitano, Elio; Xu, Jinghua; Kapadia, Suresh; Byrne, Denis; Nummy, Laurence; Grinberg, Nelu; Shen, Sherri; Lee, Heewon; Farina, Vittorio
Chimia, 2006 , vol. 60, # 9 p. 566 - 573
反应条件
1: ZnCl2 / tetrahydrofuran
2: ZnCl2
View Scheme
参考文献
Eriksson, Magnus; Napolitano, Elio; Xu, Jinghua; Kapadia, Suresh; Byrne, Denis; Nummy, Laurence; Grinberg, Nelu; Shen, Sherri; Lee, Heewon; Farina, Vittorio
Chimia, 2006 , vol. 60, # 9 p. 566 - 573
反应条件
1: CH2Cl2 / 21 h / Heating
2: CH2Cl2 / 1) 0 deg C, 5 h, 2) 25 deg C, overnight
View Scheme
参考文献
Altmann, Eva; Nebel, Kurt; Mutter, Manfred
Helvetica Chimica Acta, 1991 , vol. 74, # 4 p. 800 - 806
反应条件
in dichloromethane
1) 0 deg C, 5 h, 2) 25 deg C, overnight;
参考文献
Altmann, Eva; Nebel, Kurt; Mutter, Manfred
Helvetica Chimica Acta, 1991 , vol. 74, # 4 p. 800 - 806
